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Archive for Process

New sample changer

The Bruker Avance III 500 MHz instrument is now equipped with an automatic sample changer. The capacity of the new system is 24 samples. The new equipment will significantly optimize the use of the instrument time of one of the most demanded instruments in the Center for Magnetic Resonance.

The new instrument in the CMR

A new NMR spectrometer – Bruker AVANCE 500 NEO was launch at the Center for Magnetic Resonance. The AVANCE NEO represents the next generation in the AVANCE series product line. The AVANCE NEO is based on a ‘transceive’ principle, meaning each NMR channel has both transmit and receive capabilities. So each channel is its own independent spectrometer with the full RF generation, transmission and receive infrastructure.

This architecture provides the greatest flexibility in terms of instrument configuration and multi-channel operation. Multi-receive experiments are easily implemented with this new approach.

The spectrometer will soon be equipped with a broadband
CryoProbe™ Prodigy (BBO), which will reduce the time of long heteronuclear NMR experiments by several times and significantly
reduce the waiting time for spectral data by users.

The cryomagnet of the spectrometer is equipped with an air suspension system that reduces vibrations and, as a result, significantly improves spectrum quality.

The spectrometer operates under the latest version of TopSpin 4 software, which implements the latest advances in spectral data processing and analysis.

New external address of the CMR ftp server

The external IP address of the CMR ftp server was changed.

New address: 185.148.210.65

(Other parameters remained unchanged)

April

Total in April 2877 service applications were carried out.
All together measured:

  • 2729 1H spectra
  • 421 13C spectra
  • 130 DEPT spectra
  • 69 COSY spectra
  • 53 NOESY spectra
  • 49 31P spectra
  • 115 19F spectra

323 applications were carried out.

March

Total in March 2749 service applications were carried out.
All together measured:

  • 2596 1H spectra
  • 462 13C spectra
  • 157 DEPT spectra
  • 67 COSY spectra
  • 53 NOESY spectra
  • 111 31P spectra
  • 144 19F spectra

299 applications were carried out.

February

Total in February 2014 service applications were carried out.
All together measured:

  • 1848 1H spectra
  • 366 13C spectra
  • 87 DEPT spectra
  • 41 COSY spectra
  • 22 NOESY spectra
  • 85 31P spectra
  • 91 19F spectra

239 applications were carried out.

January

Total in January 1440 service applications were carried out.
All together measured:

  • 1294 1H spectra
  • 247 13C spectra
  • 61 DEPT spectra
  • 29 COSY spectra
  • 17 NOESY spectra
  • 72 31P spectra
  • 58 19F spectra

163 applications were carried out.

December

Total in December 2367 service applications were carried out.
All together measured:

  • 2160 1H spectra
  • 371 13C spectra
  • 96 DEPT spectra
  • 68 COSY spectra
  • 17 NOESY spectra
  • 78 31P spectra
  • 127 19F spectra

228 applications were carried out.

October

Total in October 2347 service applications were carried out.
All together measured:

  • 2218 1H spectra
  • 366 13C spectra
  • 95 DEPT spectra
  • 63 COSY spectra
  • 19 NOESY spectra
  • 52 31P spectra
  • 169 19F spectra

242 applications were carried out.

September

Total in September 1938 service applications were carried out.
All together measured:

  • 1821  1H spectra
  • 296  13C spectra
  • 72  DEPT spectra
  • 22  COSY spectra
  • 22  NOESY spectra
  • 27  31Р spectra
  • 142  19F spectra

219 applications were carried out.